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<span style="font-size: 11.0pt; font-family: '微软雅黑','sans-serif'; mso-ascii-font-family: Tahoma; mso-hansi-font-family: Tahoma; mso-bidi-font-family: 'Times New Roman'; mso-bidi-theme-font: minor-bidi; mso-ansi-language: EN-US; mso-fareast-language: ZH-CN; mso-bidi-language: AR-SA;">【标准】</span><span style="font-size: 11.0pt; font-family: 'Tahoma','sans-serif'; mso-fareast-font-family: 微软雅黑; mso-bidi-font-family: 'Times New Roman'; mso-bidi-theme-font: minor-bidi; mso-ansi-language: EN-US; mso-fareast-language: ZH-CN; mso-bidi-language: AR-SA;" lang="EN-US"><br /> <br /> </span><span style="font-size: 11.0pt; font-family: '微软雅黑','sans-serif'; mso-ascii-font-family: Tahoma; mso-hansi-font-family: Tahoma; mso-bidi-font-family: 'Times New Roman'; mso-bidi-theme-font: minor-bidi; mso-ansi-language: EN-US; mso-fareast-language: ZH-CN; mso-bidi-language: AR-SA;">根据</span><span style="font-size: 11.0pt; font-family: 'Tahoma','sans-serif'; mso-fareast-font-family: 微软雅黑; mso-bidi-font-family: 'Times New Roman'; mso-bidi-theme-font: minor-bidi; mso-ansi-language: EN-US; mso-fareast-language: ZH-CN; mso-bidi-language: AR-SA;" lang="EN-US">2020</span><span style="font-size: 11.0pt; font-family: '微软雅黑','sans-serif'; mso-ascii-font-family: Tahoma; mso-hansi-font-family: Tahoma; mso-bidi-font-family: 'Times New Roman'; mso-bidi-theme-font: minor-bidi; mso-ansi-language: EN-US; mso-fareast-language: ZH-CN; mso-bidi-language: AR-SA;">版《中国药典》配制</span><span style="font-size: 11.0pt; font-family: 'Tahoma','sans-serif'; mso-fareast-font-family: 微软雅黑; mso-bidi-font-family: 'Times New Roman'; mso-bidi-theme-font: minor-bidi; mso-ansi-language: EN-US; mso-fareast-language: ZH-CN; mso-bidi-language: AR-SA;" lang="EN-US"><br /> <br /> </span><span style="font-size: 11.0pt; font-family: '微软雅黑','sans-serif'; mso-ascii-font-family: Tahoma; mso-hansi-font-family: Tahoma; mso-bidi-font-family: 'Times New Roman'; mso-bidi-theme-font: minor-bidi; mso-ansi-language: EN-US; mso-fareast-language: ZH-CN; mso-bidi-language: AR-SA;">【名称】</span><span style="font-size: 11.0pt; font-family: 'Tahoma','sans-serif'; mso-fareast-font-family: 微软雅黑; mso-bidi-font-family: 'Times New Roman'; mso-bidi-theme-font: minor-bidi; mso-ansi-language: EN-US; mso-fareast-language: ZH-CN; mso-bidi-language: AR-SA;" lang="EN-US"><br /> <br /></span><span lang="EN-US"><span style="font-family: 微软雅黑, sans-serif;"><span style="font-size: 14.6667px;">乙二胺四醋酸二钠滴定液(0.05mol/L)</span></span><br /> <br /> </span><span style="font-size: 11.0pt; font-family: '微软雅黑','sans-serif'; mso-ascii-font-family: Tahoma; mso-hansi-font-family: Tahoma; mso-bidi-font-family: 'Times New Roman'; mso-bidi-theme-font: minor-bidi; mso-ansi-language: EN-US; mso-fareast-language: ZH-CN; mso-bidi-language: AR-SA;">【配制】</span><span style="font-size: 11.0pt; font-family: 'Tahoma','sans-serif'; mso-fareast-font-family: 微软雅黑; mso-bidi-font-family: 'Times New Roman'; mso-bidi-theme-font: minor-bidi; mso-ansi-language: EN-US; mso-fareast-language: ZH-CN; mso-bidi-language: AR-SA;" lang="EN-US"><br /> <br /> </span><span lang="EN-US"><span style="font-family: Tahoma, sans-serif;"><span style="font-size: 14.6667px;">取乙二胺四醋酸二钠19g，加适量的水使溶解成1000ml，摇匀。</span></span><br /> <br /> </span><span style="font-size: 11.0pt; font-family: '微软雅黑','sans-serif'; mso-ascii-font-family: Tahoma; mso-hansi-font-family: Tahoma; mso-bidi-font-family: 'Times New Roman'; mso-bidi-theme-font: minor-bidi; mso-ansi-language: EN-US; mso-fareast-language: ZH-CN; mso-bidi-language: AR-SA;">【标定】</span><span style="font-size: 11.0pt; font-family: 'Tahoma','sans-serif'; mso-fareast-font-family: 微软雅黑; mso-bidi-font-family: 'Times New Roman'; mso-bidi-theme-font: minor-bidi; mso-ansi-language: EN-US; mso-fareast-language: ZH-CN; mso-bidi-language: AR-SA;" lang="EN-US"><br /> <br /></span> <span style="font-family: 微软雅黑, sans-serif;"><span style="font-size: 14.6667px;">取于约800℃灼烧至恒重的基准氧化锌</span></span><span style="font-size: 14.6667px; font-family: 微软雅黑, sans-serif;">0.12g，精密称定，加稀盐酸3ml使溶解，加水25ml</span><span style="font-size: 14.6667px; font-family: 微软雅黑, sans-serif;">加0.025%甲基红的乙醇溶液1滴，滴加氨试液至溶液</span><span style="font-size: 14.6667px; font-family: 微软雅黑, sans-serif;">显微黄色，加水25ml与氨-氯化铵缓冲液(pH10.0)10ml，再加铬黑T指示剂少量，用本液滴定至溶液由紫色变为纯蓝色，并将滴定的结果用空白试验校正。</span> <span style="font-size: 14.6667px; font-family: 微软雅黑, sans-serif;">每1ml乙二胺四醋酸二钠滴定液(0.05mol/L)相当于</span><span style="font-size: 14.6667px; font-family: 微软雅黑, sans-serif;">4.069mg的氧化锌。</span> <span style="font-size: 14.6667px; font-family: 微软雅黑, sans-serif;">根据本液的消耗量与氧化锌的取</span><span style="font-size: 14.6667px; font-family: 微软雅黑, sans-serif;">用量，算出本液的浓度，即得。</span> <span style="font-size: 11.0pt; font-family: '微软雅黑','sans-serif'; mso-ascii-font-family: Tahoma; mso-hansi-font-family: Tahoma; mso-bidi-font-family: 'Times New Roman'; mso-bidi-theme-font: minor-bidi; mso-ansi-language: EN-US; mso-fareast-language: ZH-CN; mso-bidi-language: AR-SA;">【贮存】</span><span style="font-size: 11.0pt; font-family: 'Tahoma','sans-serif'; mso-fareast-font-family: 微软雅黑; mso-bidi-font-family: 'Times New Roman'; mso-bidi-theme-font: minor-bidi; mso-ansi-language: EN-US; mso-fareast-language: ZH-CN; mso-bidi-language: AR-SA;" lang="EN-US"><br /> <br /></span><span style="font-family: 微软雅黑, sans-serif;"><span style="font-size: 14.6667px;">置玻璃塞瓶中，避免与橡皮寒、橡皮管等接触。</span></span> <span style="font-size: 11.0pt; font-family: '微软雅黑','sans-serif'; mso-ascii-font-family: Tahoma; mso-hansi-font-family: Tahoma; mso-bidi-font-family: 'Times New Roman'; mso-bidi-theme-font: minor-bidi; mso-ansi-language: EN-US; mso-fareast-language: ZH-CN; mso-bidi-language: AR-SA;">中国药典产品发布参考示例</span> |
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