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<span style="font-size: 11.0pt; font-family: '微软雅黑','sans-serif'; mso-ascii-font-family: Tahoma; mso-hansi-font-family: Tahoma; mso-bidi-font-family: 'Times New Roman'; mso-bidi-theme-font: minor-bidi; mso-ansi-language: EN-US; mso-fareast-language: ZH-CN; mso-bidi-language: AR-SA;">【标准】</span><span style="font-size: 11.0pt; font-family: 'Tahoma','sans-serif'; mso-fareast-font-family: 微软雅黑; mso-bidi-font-family: 'Times New Roman'; mso-bidi-theme-font: minor-bidi; mso-ansi-language: EN-US; mso-fareast-language: ZH-CN; mso-bidi-language: AR-SA;" lang="EN-US"><br /> <br /> </span><span style="font-size: 11.0pt; font-family: '微软雅黑','sans-serif'; mso-ascii-font-family: Tahoma; mso-hansi-font-family: Tahoma; mso-bidi-font-family: 'Times New Roman'; mso-bidi-theme-font: minor-bidi; mso-ansi-language: EN-US; mso-fareast-language: ZH-CN; mso-bidi-language: AR-SA;">根据</span><span style="font-size: 11.0pt; font-family: 'Tahoma','sans-serif'; mso-fareast-font-family: 微软雅黑; mso-bidi-font-family: 'Times New Roman'; mso-bidi-theme-font: minor-bidi; mso-ansi-language: EN-US; mso-fareast-language: ZH-CN; mso-bidi-language: AR-SA;" lang="EN-US">2020</span><span style="font-size: 11.0pt; font-family: '微软雅黑','sans-serif'; mso-ascii-font-family: Tahoma; mso-hansi-font-family: Tahoma; mso-bidi-font-family: 'Times New Roman'; mso-bidi-theme-font: minor-bidi; mso-ansi-language: EN-US; mso-fareast-language: ZH-CN; mso-bidi-language: AR-SA;">版《中国药典》配制</span><span style="font-size: 11.0pt; font-family: 'Tahoma','sans-serif'; mso-fareast-font-family: 微软雅黑; mso-bidi-font-family: 'Times New Roman'; mso-bidi-theme-font: minor-bidi; mso-ansi-language: EN-US; mso-fareast-language: ZH-CN; mso-bidi-language: AR-SA;" lang="EN-US"><br /> <br /> </span><span style="font-size: 11.0pt; font-family: '微软雅黑','sans-serif'; mso-ascii-font-family: Tahoma; mso-hansi-font-family: Tahoma; mso-bidi-font-family: 'Times New Roman'; mso-bidi-theme-font: minor-bidi; mso-ansi-language: EN-US; mso-fareast-language: ZH-CN; mso-bidi-language: AR-SA;">【名称】</span><span style="font-size: 11.0pt; font-family: 'Tahoma','sans-serif'; mso-fareast-font-family: 微软雅黑; mso-bidi-font-family: 'Times New Roman'; mso-bidi-theme-font: minor-bidi; mso-ansi-language: EN-US; mso-fareast-language: ZH-CN; mso-bidi-language: AR-SA;" lang="EN-US"><br /> <br /> </span><span lang="EN-US"><span style="font-family: Tahoma, sans-serif;"><span style="font-size: 14.6667px;">烃铵盐滴定液(0.01mol/L)</span></span><br /> <br /> </span><span style="font-size: 11.0pt; font-family: '微软雅黑','sans-serif'; mso-ascii-font-family: Tahoma; mso-hansi-font-family: Tahoma; mso-bidi-font-family: 'Times New Roman'; mso-bidi-theme-font: minor-bidi; mso-ansi-language: EN-US; mso-fareast-language: ZH-CN; mso-bidi-language: AR-SA;">【配制】</span><span style="font-size: 11.0pt; font-family: 'Tahoma','sans-serif'; mso-fareast-font-family: 微软雅黑; mso-bidi-font-family: 'Times New Roman'; mso-bidi-theme-font: minor-bidi; mso-ansi-language: EN-US; mso-fareast-language: ZH-CN; mso-bidi-language: AR-SA;" lang="EN-US"><br /> <br /> </span> <span style="font-family: Tahoma, sans-serif;"><span style="font-size: 14.6667px;">取氯化二甲基苄基烃铵3.8g，加水溶解后，</span></span><span style="font-size: 14.6667px; font-family: Tahoma, sans-serif;">加醋酸-醋酸钠缓冲液(pH3.7)10ml，再加水稀释成1000ml，摇匀。</span> <span style="font-size: 11.0pt; font-family: 'Tahoma','sans-serif'; mso-fareast-font-family: 微软雅黑; mso-bidi-font-family: 'Times New Roman'; mso-bidi-theme-font: minor-bidi; mso-ansi-language: EN-US; mso-fareast-language: ZH-CN; mso-bidi-language: AR-SA;" lang="EN-US"> <br /> </span><span style="font-size: 11.0pt; font-family: '微软雅黑','sans-serif'; mso-ascii-font-family: Tahoma; mso-hansi-font-family: Tahoma; mso-bidi-font-family: 'Times New Roman'; mso-bidi-theme-font: minor-bidi; mso-ansi-language: EN-US; mso-fareast-language: ZH-CN; mso-bidi-language: AR-SA;">【标定】</span><span style="font-size: 11.0pt; font-family: 'Tahoma','sans-serif'; mso-fareast-font-family: 微软雅黑; mso-bidi-font-family: 'Times New Roman'; mso-bidi-theme-font: minor-bidi; mso-ansi-language: EN-US; mso-fareast-language: ZH-CN; mso-bidi-language: AR-SA;" lang="EN-US"><br /> </span> <span style="font-family: Tahoma, sans-serif;"><span style="font-size: 14.6667px;">取在150℃干燥1小时的分析纯氯化钾约</span></span><span style="font-size: 14.6667px; font-family: Tahoma, sans-serif;">0.18g，精密称定，置250ml量瓶中，加醋酸-醋酸钠缓冲液(pH3.7)使溶解并稀释至刻度，摇匀，精密量取</span><span style="font-size: 14.6667px; font-family: Tahoma, sans-serif;">20ml置50ml量瓶中，精密加人四苯硼钠滴定液(0.02mol/L)25ml，用水稀释至刻度，摇匀，经干燥滤纸</span><span style="font-size: 14.6667px; font-family: Tahoma, sans-serif;">滤过，精密量取续滤液25ml，置150ml锥形瓶中，加溴酚蓝指示液0.5ml，用本液滴定至蓝色，并将滴定的结果</span><span style="font-size: 14.6667px; font-family: Tahoma, sans-serif;">用空自试验校正，每1ml烃铍盐滴定液(0.01mol/L)相当于0.7455mg的氯化钾。</span> <span style="font-size: 11.0pt; font-family: '微软雅黑','sans-serif'; mso-ascii-font-family: Tahoma; mso-hansi-font-family: Tahoma; mso-bidi-font-family: 'Times New Roman'; mso-bidi-theme-font: minor-bidi; mso-ansi-language: EN-US; mso-fareast-language: ZH-CN; mso-bidi-language: AR-SA;">中国药典产品发布参考示例</span> <span style="font-size: 11.0pt; font-family: 'Tahoma','sans-serif'; mso-fareast-font-family: 微软雅黑; mso-bidi-font-family: 'Times New Roman'; mso-bidi-theme-font: minor-bidi; mso-ansi-language: EN-US; mso-fareast-language: ZH-CN; mso-bidi-language: AR-SA;" lang="EN-US"> <!--[if !supportLineBreakNewLine]--><br /> <!--[endif]--></span> |
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